Based on Jim DeKorne's "Psychedelic Shamanism"
DeKorne says he discovered that you could make a smokable extract by accident, after leaving an extract intended for ayahuesque use out where the alcohol evaporated, leaving "a gummy tar" which he "on a sudden whim" decided to smoke. "I took one inhalation of this essence and found my mind immediately blasted into a cerebral hurricane of rapidly pulsing white light. Fortunately, I already knew what a DMT flash is like, so I was not totally taken by surprise."
His idea of extraction is this:
As a footnote, he tried similar stuff with Arundo donax and got some really nasty reactions from whatever other crud was in the plant. I'm gonna cross this one off of my list.
His idea of extraction is this:
- Pulverize the grass clippings
- Add water, "enough... to make a pourable soup"
- Acidify to pH 5 or so
- (Optional) Simmer the acidified soup in a slow cooker overnight, not allowing the liquid to evaporate. ("It may take two or three such operations to get all of the alkaloids into solution")
- Strain the plant matter through cheesecloth, then through a paper coffee filter
- Add 10-15% of the mass of the solution in a "defatting solvent" such as methylene chloride, ether, chloroform, or naptha. [Be extremely careful about the use of naptha]
- Shake vigorously
- The crap will go into the solvent, leaving the good stuff in the water.
- Separate the water from the solvent.
- Add a base to the aqueous solution in small increments until the pH gets to about 9 or 10. This converts the alkaloids into their free base.
- Extract with 10% of the mass of the solution of an organic solvent four times, at one 24-hour and then three weekly intervals. The solvent layer will take on a darker tint, usually yellowish or reddish-brown. It will take almost a month to extract all of the alkaloids, and the solution should be shaken at least twice a day between extractions.
- Evaporate the solvent off from the combined extract fractions. You now have the alkaloids.
As a footnote, he tried similar stuff with Arundo donax and got some really nasty reactions from whatever other crud was in the plant. I'm gonna cross this one off of my list.